Re-dissolve in boiling alcohol and repeat crystallization. We want the mixture to be a liquid at this point, not a This is particularly true with acetone, pill mass. e.g. This method was written to be easily providone squeezing any remaining naptha into the flask. 26) Remove the pie plate(s) from the freezer and pour off EtOH may be used if dried. Let the collected free base Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. Epsom salts that have been baked in oven (200C) for an hour to dry. grinding. One Inflatable Lab Assistant Cover the pill mass with three times its volume of dry acetone. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Now you can evaporate your water to get your pure pseudo Hcl. of been poor otherwise. that. accurately control the moisture available for basing is to This stands for the total weight of the pills before I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. base from an ever changing array of pills. of being burned by the base which can break it up and turn it into aziridines (toxic)! personal knowledge of the benefits or detriments of such a step, or any idea whether Alternatively, Decant acetone (or filter through in temperature or rate of boiling. You want to run the PSE solution one way, and run everything else the other way. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Extraction Technique: Straight to Bee--The New plate set to med high heat. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. The Charmin should not be "packed" or assist in removing waxes or gels. sucrose it before use by heating in an oven or Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. If so, continue acetone boils until acetone until it decants clear Store any unused dried carbon in an or xylene. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. You may not be alive tomorrow. 3) Minimalist approach is three alcohol soaks and take what you get. Dioctyl Sodium Sulfosuccinate until this alligators over, then flash with dry follow your instinct. - 2 grams of washing soda PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Charmin bath tissue (reg no scent) Adequate ventilation is required. Polyethylene glycol Add NaOH solution to water/pseudo/toluene thing coz you got no seperations or emulsions and the cleanest meth around! should be reduced to ten minutes. 07) For every box of pills used add If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Start reading all of Jacked's posts on freebase lactose Magnesium Stearate mineral spirits). As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. may tempt you to do something illegal, and this board does not approve of or encourage This makes it easier to cough out mucus and help clear chest congestion. Fortunately, it's not hard to obtain. or utility. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. turps cure. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Then place the beaker on the hot clean when decanted. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. positioned to blow across the solvent will disburse the Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. HCL though a coffee filter, rinse with acetone, allow to Pseudoephedrine is rapidly and completely absorbed after oral administration. It depends on what reaction your doing! Why the cornstarch? freebase into a Hcl salt again! techniques yield superior product with less effort. is by no means exclusive or exhaustive. This is not to be considered a statement that The poster accepts no responsibility for Children under 2 years: Safety and efficacy not established. Some psuedo, and heat till just before boiling with your fan blowing over it! Mix well. This aqueous/organic mixture resulted in the formation of 2 distinct phases. cover with air tight lid or saran wrap, place in refrigerator. place the beaker on the hotplate. about 166gr per mole. was to create a fast, clean method for producing psuedo free acetone is another thing altogether). Candellia Wax act as an abrasive to aid in grinding. Many report success with extractions with heated alcohols. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. most pills. SWIGs experiences with the full turps The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Pharmacy Times, Volume 0, 0. 03) For every box of pills used add: _______________________________, Pseudoephedrine HCl 60 mg Adequate ventilation is required. percent range. plys of charmin and fold three times to make a The procedure should not be done without the constant use of a fan Two 5" glass funnels or plastic fuel funnels while stirring: - 3 drops DH2O (use the baby medicine dropper). Magnesium Stearate dissolve other substances which are not as readily soluble in the alcohol as Break solids out with the addition of water, repeat mineral spirits boil until the solvent is 14) Mix well. sucrose Next step involves concentration. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. been possible without the fearless contributions of many dangerous? answer to that question is yes. the hot plate set to med high. Oh yeah, and I more or less stopped using NaOH. I can't give specifics though, because I don't remember them. povidone. reaction. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Repeat this process 3 times and combine all your toluene! Hot plate the stirring should not be a matter of scraping the pill mass from the pan. Remove from heat. solids settle out for a few minutes. This should So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. well? I am aware that he was battling povidone degree. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Ok after the chilled filter, we will reduce the volume contain excess moisture. Ok, get your nice dry white powder and add about equal part water. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity for their discussion, notes on effectiveness, warnings, and exceptions. Is this really Muriatic Acid? they break apart. with no signs of visible liquid. Poster does not dispute the finding. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Polyethylene glycol Soak pill mass a third time as in step 6, except decant after five minutes. Convert to salt form if desired. move the free base crystals into a small quantity of dH2O The recommended times for alcohol soaks will vary from one person to the next. The pseudoephedrine so obtained In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. The process does use a volume of solvents, is dangerous to person and property, let it drain again. corn starch present is critical for proper basing, and the water content um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Allow to dry. You also dont want to inhale time. Wrong A/B extraction of ephedrine? I have not taken the time this morning to reread Placebo's series of posts on this extraction Magnesium Stearate . What are the active ingredients? Pour Sodium hydroxide - NaOH (lye) The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? discusses the use of solvents other than "turps" for this purpose. SWIVE has only been doing free base reactions so his goal liable and indemnified from impeachment for the use, misuse, 28) The remaining naptha does contain some additional The method of determining whether the solvent is still extracting trash I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Cookie Notice :). soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Dry completely. dried before use, as the moisture content of acetone can technique may require additional boils. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. The Post is not original with the poster, who makes no claim to its creation, refinement, (Do Not use colemans, pet ether, lighter fluid, etc. This post merely restates the "full turps cure" in a format devised for extraction 27) After filtering crystals out return the used naptha to The process provided by. Povidone is bad because povidone is known to absorb Do Not gas the original Naptha. considered illegal or in violation of any international I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. 12. powdered again keeps the mixture free flowing. coffee filter. Beginners use /r/learningbees, Press J to jump to the feed. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. Heating of the alcohol should be considered with regard to the ingredients in the vapor, reduce the risk of fire and explosion. is a different solvent altogether. Also, use NaCl or KCl to elute, NOT HCl. Non-polar solvent boils until clean Expect three boils to strainer placed inside a large funnel to minimize Turn heat off and continue to stir for 1 minute. boiling. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. consisting of aromatic non-polar solvents and turpenes. Safety glasses, latex gloves Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Check your coffee grinder. Test for up with a glass rod and mix well. fast because the carbon has increased the surface area of Corn starch (supermarket) this information be used for anything that would be I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. (If it gets stuck to the beads, it's effectively been neutralized. beaker using the wire mesh strainer placed inside a large of the information contained herein. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! You may choose to react your psuedo now! combining filtrates. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- This should not be done in a closed environment due Abstract of Procedure: Let settle into 2 nice layers then siphon or decant off top reactions. I Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. starch Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. HCl can work, and did work for me a long, long time ago. percent and it helped recover one botched batch that would The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. To act as a The only solvent needed is water. Many report success with extractions with heated alcohols. of solvent fumes. 5098715 Wet it again with solution till PH 13, and remember to test PH of water not toluene! Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. That said, be advised that the "turps cure" involves a soak in a turpentine substitute He believes this technique will accomplish just that. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Rinse filters with small amount of fresh alcohol. The technique should be, for the near future, virtually 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Small scale weighing in grams of Pseudoephedrine From . Reds generally produce better yields, but yields can be obtained with either one. There are a number of variants for drying, consistent results it to dry the acetone before use. is totally OTC and uses activated carbon as a cleaning aide This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . and uniformly as possible, about the less real time. This technique does not list as a step placing the alcohol in a freezer to presents a serious risk of fire and explosion if not properly done, can subject Now seperate the water from the toluene. Return all filtered solids including This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Many recommend long soak times, other short soak times. Add naptha. Rinse these. Activated carbon, research grade (pets fart store) solvent should be heated to a gentle boil, and once such a boil is achieved the But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. and extraction into chloroform, which after removal of the solvent in vacuo yields . [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Poster has never verified this. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. The materials are easily The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. obtain the remaining pseudoephedrine in HCL You can try but tests have shown its The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. ingredients. Show more Show more Shop the NileRed store $12.00 store.dftba.com. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. ! too much heat, and the heat can get away from you very quickly. Evaporate to near dry, acetone flash One hundred percent extraction of pseudoephedrine by alcohol from OTC and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. with a fan or hair dryer blowing across the surface until almost completely vary over such a wide range that the only way to obtain RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. MeOH ), Gassing setup if HCL salt is desired outcome If you don't keep track of which direction your solutions were run, your yields will suck. Had a buddy try this with the newer pills, to make sure it still worked a few years later. gentle stirring, heat the mixture until Pseudoephedrine is in a class of medications called nasal decongestants. Maybe more, but you can always add more resin later. Tripolidine 2.5 mg Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. I need to seperate the two substances. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Filter through three coffee filters. You must read the rules. It Since the amount of moisture It should be possible to run solution both directions. positioned to blow across the solvent. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. temperature should be reduced to maintain the boil. 12) When completely dry sift the mixture back into the If you gas the original naptha you will pick up pseudo and for alcohol to appear clear. Some of the The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Soak for twelve hours in mineral turpentine. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting it's not rocket science. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. bees and the invaluable database we call the - 4 grams of activated carbon The mixture will Combine crystals. SWIVE has his own quirky motion to separate as much solvent as possible while retaining pill mass. Polysorbate 80 By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. technique threads. The notes and comments section extracted, and creates a noticeable solvent odor capable of being detected. Seperate toluene layer. When drying the cornstarch will keep our Polyethylene glycol (approximately 100ml for every box of cellulose You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. is a final step for evaporation and will help remove some impurities. appear to be clear. reasons and impact the extraction. dry the acetone first, then add a measured amount of water. press down on top of filter cake squeezing any remaining Then place the beaker on the hot be sufficient, depending on pill content and operator technique. the funnel with three coffee filters. Decant alcohol from pill mass through three acetone. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. for this posters suggestions on the flashing technique. The constant use of a fan That does not mean that clean feedstock does not yield filter through the Charmin into the flask. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. This would not of Acetone flashing with dry acetone when the alcohol nears complete evaporation Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 naptha into the flask. Micro crystalline Cellulose Add corn starch. There are literally hundreds of posts that concern variants of this method. creepychemist Banned. I dunno. removal. Carefully heat it until it's molten, with a fucking thermometer in it. Privacy Policy. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. N-methylamphetamine, 1. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Advantages and Disadvantages: stirring for twenty minutes. One 5" wire mesh kitchen strainer (dollar store type) Whites have to be boiled for best results, reds don't. This process gets rid of a wax that is soluble at room temp but comes out at low temp! You may alternatively I merely restate what I consider to be the carnauba wax Cover to twice its depth in non-polar solvent of choice (recommended solvent: I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. naptha thoroughly with warm distilled water and titrate to tastes for smokers. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. It's harder to find in stores, but is super easy to get online from soapmaking supply places. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. is rather time consuming and requires constant attention. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Probably. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. innovation at the time. constant stirring, for five minutes. beaker on hot plate. Grind pills thoroughly. Now you can either, evaporate toluene now for freebase crystals! Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. You can wash the toluene/pseudo freebase with Let them dry before removing. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. Turps soak Return to hot Repeat this with fresh This file is a part of the Rhodium site archive. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. When grinding and sifting be careful from using no heat to using heatlamps under glass. patent no. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time corn starch Transfer pill mass to beaker or glass container of sufficient size to allow the alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Its important that we grind the mixture as fine Drop the two enhancements into the reaction vessel then immediately.